In need of good SAXS? You can now collaborate with us (like a mini-“large facility”)!

CC0-licensed cheesy image of collaboration from: https://pxhere.com/en/photo/1445429
CC0-licensed cheesy image of collaboration from: https://pxhere.com/en/photo/1445429

If you are in need of good small- or wide-angle X-ray scattering insights to further your projects, I am happy to say that we can now help you! We can offer a guided experience where we will assist in the planning, measurement, correction, analysis and interpretation of all your scattering-related questions, suitable for experts and beginners alike. Read on below to find out how…

Why do you do this?

CC0-licensed cheesy image of collaboration from: https://pxhere.com/en/photo/1445429
CC0-licensed cheesy image of collaboration from: https://pxhere.com/en/photo/1445429

BAM, is a government-funded institute, whose primary goal is to help industry and academia answer their materials-related questions. To achieve this, BAM invests (amongst others) in instruments, and – more importantly – people with years of associated expertise. We spend part of our time improving our knowledge by doing our own research, but we are also available for collaborations within, and on the boundaries of our expertise.

That means that you do not need to buy expensive equipment to do your occasional specialized experiment, and that you do not need to spend years developing the knowledge necessary to make correct educated guesses on what your techniques are really telling you. Instead, you can bring your questions to us. As mentioned in my last post, such collaborations really benefit both you and us equally: you get help with the application of an interesting, yet challenging technique, and we get better insights on how to answer a very wide range of questions (as well as the occasional co-authorship, see below).

Types of collaborations

So, to put it more concretely, if you are doing materials science, and you want to add a SAXS or WAXS investigation to your analyses, you can contact us. Or, if you are in, or near Berlin, drop by for a chat! We will quickly find out if your experiment is feasible on our top-of-the-line lab instrument, or if you really need the special powers that a synchrotron has to offer. If our labs will do, we can collaborate in one of three ways:

  1. Industrial collaborations: If you need the investigation for an internal research project, and the investigations are not intended for public release, industrial collaborations are the choice for you. In this case, we will happily help you out for a standardized fee.
  2. Research collaborations: As a government institute, BAM is eligible to apply for special sources of funding, such as DfG or special EU funds. We are always happy to join such (and other) funding applications as a partner. This is particularly useful for larger research projects.
  3. Basic research: This is the option we have been exploring in the past few months, and has now become available. If you have a research project and you need us, we may help you with all SAXS/WAXS aspects of your research, including some interpretation. Co-authorships on the papers where we have provided an intellectual contribution are expected, and indeed very helpful, as they allow us to justify this way of working.
  4. Bonus option: If you are a student, you can also do a Bachelor, Master, Ph.D. or Post-doc project in our labs. You do need a university supervisor, but we do host a legion of excellent students and post-docs throughout BAM. We particularly appreciate it if you come with your own project plans. More info here.

So do you accept everything?

Unfortunately not. We are limited in measurement time and our staff time, so we can only accept some projects, and we will ramp up slowly over the next few months. Until we are oversubscribed, we will only check project and collaboration proposals for technical feasibility, as well as our group emphases (protein scattering, for example, is at the moment not one of our core expertise). We also make a prioritization of measurements, but we typically manage to return most samples within two weeks.

Once we start getting oversubscribed, we will start with frequent calls for proposals with regular deadlines. Proposals in this case are very brief excel sheets where a little basic information can be provided. Examples will follow shortly.

For researchers abroad, there is also the option mailing in the samples, saving a ton of CO2 and money.

What samples can you measure?

There will be a more extensive gallery later, but here’s a brief cross-section on what we can measure:

  • Nanoparticles in solid- or liquid dispersion
  • Porous materials, including: SBA, MOFs, membranes, fibres
  • Polymer materials, both amorphous and (semi-)crystalline
  • Precipitates in alloys (aluminium-, magnesium-based alloys or steels in particular)
  • Composite materials
  • Glassy materials
  • milk, ink, water, etc.
  • Some deposited surfaces as well, although we do not have much experience yet with grazing incidence.
  • A variety of other powders, sheets, films, liquids, gels,

We haven’t got many in-situ set-ups yet, but we are expanding based on need. We expect soon to be able to do:

  • in-situ heating to moderate temperatures (< 500 ˚C), also with fast ramp rates
  • in-situ tensile testing
  • flow-through sampling of reactions
  • measurements under moderate, static magnetic fields (< 0.5 T)

We specialize in:

  • Wide-range measurements of static samples, from 0.02 < q(1/nm) < 90. Soon to be extended with USAXS, adding the range of 0.002 < q(1/nm) < 0.02.
  • calibrated measurements, absolute units and uncertainties on the intensity, traceable Q-vector calibration
  • full data correction method developments
  • advanced analysis method developments
  • complex samples
  • aligned, anisotropic structures
  • medium- to slow dynamics studies (to study processes lasting up to several weeks, with time steps of several minutes), such as room-temperature ageing studies or slow synthesis reactions.

We cannot do:

  • Weakly scattering samples
  • Anomalous scattering investigations
  • fast dynamics investigations
  • highly absorbing or thick samples
  • high-resolution diffraction
  • samples under atmosphere

Is it just the MAUS you’re sharing?

For the Basic Research-type of sharing, yes, until we demonstrate that this way of working makes sense. For the Industrial Collaborations and Research Collaborations, we have more equipment available, including another flow-through SAXS machine and an advanced multi-angle static- and dynamic light scattering machine.

Will there be paperwork?

Only the bare minimum. A little bit of paperwork cannot be avoided. On top of that, we need some paperwork to correctly register your samples and measurements.

So is this all you do now?

No, we mainly do research for ourselves and our group, and we assist other BAM researchers with their projects too. Besides these, however, there is still plenty of capacity on the machine available, and we can usually spend a moment or two providing a judgmental look on the resulting data. We think we can do some pretty amazing measurements, so now we’re cross-checking this assumption with the rest of the world.

Let’s find out how good we really are!

P.S. is any of this legally binding?

No. This is a personal weblog. What I write here is only what I understand, and I only speak for myself (even when I use the royal “we”). I cannot guarantee that it is a correct interpretation, and so some details might not be correct. I do try to be correct, though!

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